Journal
INORGANIC CHEMISTRY
Volume 58, Issue 19, Pages 12854-12858Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.inorgchem.9b01798
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Funding
- Knut and Alice Wallenberg Foundation through 3DEM-NATUR [2012.0112]
- Swedish Research Council (VR) [2014-06948, 2017-04321]
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-ACO2-06CH11357]
- ExxonMobil Research and Engineering
- Swedish Research Council [2014-06948, 2017-04321] Funding Source: Swedish Research Council
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A new aluminosilicate zeolite, denoted EMM-37, with a 3D small pore channel system, has been synthesized using a diquaternary ammonium molecule as the structure directing agent (SDA) and metakaolin as the aluminum source. The structures of both as-made and calcined forms of EMM-37 were solved and refined using continuous rotation electron diffraction (cRED) data. cRED is a powerful method for the collection of 3D electron diffraction data from submicron- and nanosized crystals, which allows for successful solution and refinement of complex structures in symmetry as low as P (1) over bar.
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