Journal
CHEMICAL PHYSICS LETTERS
Volume 730, Issue -, Pages 354-360Publisher
ELSEVIER
DOI: 10.1016/j.cplett.2019.06.034
Keywords
Lithium-rich materials; Co-precipitation method; Oxalic acid
Funding
- Nature Science Foundations of Hebei Province [B2016210071]
- Natural Science Foundation of Hebei Education Department [QN2016057]
- National College Students' Innovative Entrepreneurial Training Project of China
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Co-precipitation method employing two precipitants, oxalic acid and ammonium oxalate, has been used to synthesize Li1.2Ni0.13Co0.13Mn0.54O2. Various calcination temperatures are also compared to obtain the material with better properties. By optimizing the precipitant and calcination temperature, the material prepared by oxalic acid at 900 degrees C has good layered structure, small particle size (200-300 nm), and uniform distribution of particles. A high first discharge specific capacity of 298.4 mAh g(-1) and a high first Coulombic efficiency of 77.2% at 0.1 C are obtained. After 50 cycles, the reversible discharge specific capacity is 272.2 mAh g(-1) with a capacity retention of 91.2%.
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