4.7 Article

Fabrication and properties of newly developed Ti35Zr28Nb scaffolds fabricated by powder metallurgy for bone-tissue engineering

Journal

JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 8, Issue 5, Pages 3696-3704

Publisher

ELSEVIER
DOI: 10.1016/j.jmrt.2019.06.021

Keywords

Corrosion resistance; Mechanical property; Porous Ti35Zr28Nb scaffold; Powder metallurgy; Pore characterization

Funding

  1. National Natural Science Foundation of China [51874037]
  2. 13th Five-Year Weapons Innovation Foundation of China [6141B012807]
  3. State Key Lab of Advanced Metals and Materials, University of Science and Technology Beijing [2019-Z14]
  4. National Health and Medical Research Council (NHMRC), Australia [GNT1087290]

Ask authors/readers for more resources

A newly developed porous Ti35Zr28Nb scaffold was manufactured via powder metallurgy (PM) using space-holder (NH4HCO3) sintering from pre-alloyed powder. The pore features, compression and anti-corrosion properties of the manufactured porous scaffolds were systematically studied. The results show that all the manufactured porous Ti35Zr28Nb scaffolds consisted of a single beta phase. The porosity of the porous Ti35Zr28Nb scaffolds increased from 50% to 65% with in increasing the NH4HCO3 from 63% to 79% (volume ratio), and the aver- age pore size (d(50)) was in the range of 230-430 mu m. The yield strength in compression and the elastic modulus of the porous Ti35Zr28Nb scaffolds both decreased gradually with an increase in porosity, varying from 230.5 MPa to 79.7 MPa and 6.9 GPa to 1.8 GPa, respectively. The corrosion rate of the porous Ti35Zr28Nb scaffolds in the phosphate buffer saline (PBS) solution increased from 0.91 x 10(-3 )mm/yr to 4.18 x 10(-3) mm/yr with an increase in porosity from 51.4% to 64.9%. In comparison with unalloyed Ti scaffolds with almost the same porosity, the porous Ti35Zr28Nb scaffolds showed a significantly higher compressive yield strength and a lower corrosion rate. These results suggest that porous Ti35Zr28Nb scaffolds fabricated by PM have substantial potential for hard-tissue engineering applications. Additionally, the relationship of porosity, mechanical and anti-corrosion properties of these Ti35Zr28Nb scaffolds has now been confirmed, and could be used in the process of material selection for their specific applications. (C) 2019 The Authors. Published by Elsevier B.V.

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