Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 84, Issue 9, Pages 5305-5312Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b00300
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Funding
- National Natural Science Foundation of China [21602046]
- MOST of China [2016YFE0132600]
- Doctor's Scientific Research Foundation of Henan University of Chinese Medicine [BSJJ2016-12]
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Various amidated nitrones were efficiently achieved through Ir(III)-catalyzed direct C-H amidation of nitrones with good to excellent yields and tolerance of broad functional groups. This reaction smoothly proceeded at room temperature in the absence of acid or base in a short reaction time. Carbon dioxide was generated as the sole byproduct, thus providing an environmentally benign amidation process. The title products could be efficiently transformed to substituted benzisoxazoline.
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