4.3 Article

Use of Ionic Liquid as Template for Hydrothermal Synthesis of the MCM-41 Mesoporous Material

Journal

SILICON
Volume 12, Issue 2, Pages 289-294

Publisher

SPRINGER
DOI: 10.1007/s12633-019-00121-9

Keywords

Ionic liquid; Template; Mesoporous material; MCM-41

Funding

  1. FAPESP (Research Support Foundation of the State of Sao Paulo) [2014/05679-4, 2017/06775-5, 2015/00609-0, 2018/18894-1]
  2. CAPES (Coordination for the Improvement of Higher Education Personnel) [309342/2010-4]
  3. CDMF (Center for the Development of Functional Materials) [2013/07296-2]
  4. Fundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP) [18/18894-1] Funding Source: FAPESP

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In this study the MCM-41 mesoporous material was first prepared by using hydrothermal method in the presence of 1-butyl-2,3-dimethylimidazolium hexafluorophosphate ([BMMIM]PF6) ionic liquid (IL) as template. The IL presented the average yields between 67 and 76%. The obtained MCM-41 showed the main structural parameters associated with the formation of condensed silica (Si - O - Si), a hexagonal mesostructure with a compact arrangement of cylindrical tubes and agglomerated spherical particles.

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