Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 358, Issue 12, Pages 1942-1945Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201600147
Keywords
aerobic conditions; alkenyl oximes; tert-butyl nitrite; metal-free procedure; nitrooxylation
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Funding
- National Natural Science Foundation of China [NSFC 21404096, U1463202]
- Fundamental Research Funds for the Central Universities of China [WK2060190022, WK2060190026, WK3430000001]
- Anhui Provincial Natural Science Foundation [1608085MB24]
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A metal-free aerobic autoxidative nitrooxylation of alkenyl oximes mediated by tert-butyl nitrite is described. Molecular oxygen is used as the oxidizing reagent, avoiding use of organic trapping reagents such as 2,2,6,6-tetramethylpiperidine 1-oxyl (TEMPO). The desired products were obtained in generally high yields.
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