Journal
ADVANCED ENGINEERING MATERIALS
Volume 19, Issue 5, Pages -Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adem.201600329
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Funding
- National Basic Research Program of China [2011CB605803]
- Advanced Nonferrous Metal Structural Materials and Manufacturing Collaborative Innovation Center
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Carbon/carbon (C/C) composites plate is prepared in the temperature range 1 223-1 373 K by improved pressure-gradient chemical vapor infiltration (CVI). The bulk densities and pore distributions of C/C composites after different infiltration period are measured and the densification kinetics is investigated. The results show that C/C composites plate with 300 x 300 x 15 mm is able to be densified to 1.52 g cm(-3) within 60 h by pressure-gradient CVI. The porosity of pores with a size larger than 60 mu m reduces markedly and the large pores are able to be filled more effectively by pressure-gradient CVI. The densification kinetics depends on the temperature and competition between reaction and convection mass transport. The activation energy is about 366 kJ mol(-1) at 1 223-1 313 K and 43.2 kJ mol(-1) above 1 313 K.
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