Journal
ORGANIC LETTERS
Volume 21, Issue 2, Pages 345-349Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b03193
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Funding
- National Program on the Key Research Project [2016YFA0602900]
- National Natural Science Foundation of China [21420102003]
- Guangdong Natural Science Foundation [2018B030308007]
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A transition-metal-free three-phase four-component coupling reaction (3P-4CR) involving KCl, arynes, chloroalkanes and CO2 has been reported for the first time, enabling the incorporation of both chloro and CO2 into an aryne simultaneously. The reactions for the synthesis of different types of o-chloro benzoates can be selectively modulated by the chloroalkane utilized. The corresponding products can be alternatively transformed for postsynthetic functionalizations conveniently.
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