Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 83, Issue 24, Pages 15170-15177Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.8b02450
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- Rhineland-Palatinate Center for Natural Product Research
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The natural 3-decalinoyltetramic acid epi-trichosetin was synthesized in ten steps starting from (R)-(+) -citronellal using an intramolecular Diels-Alder reaction and a Lacey-Dieckmann cyclization as the key steps. The use of a 2-nitrobenzyl protecting group resulted in an efficient synthetic endgame. The natural product was obtained in 4.1% overall yield.
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