4.7 Article

The combined effects of grain and sample sizes on the mechanical properties and fracture modes of gold microwires

Journal

JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
Volume 35, Issue 1, Pages 76-83

Publisher

JOURNAL MATER SCI TECHNOL
DOI: 10.1016/j.jmst.2018.09.012

Keywords

Gold microwire; Wire bonding; Tensile testing; Grain size; Hall-Petch relationship

Funding

  1. National Key R&D Program of China [2017YFA0204403]
  2. Shenzhen Virtual University Park [R-IND1710]
  3. Innovation and Technology Commission via the Hong Kong Branch of National Precious Metals Material Engineering Research Center
  4. Research Grants Council of the Hong Kong Special Administrative Region, China [CityU 11209914]
  5. General Research Fund of Hong Kong [CityU 11247516]
  6. National Natural Science Foundation of China [51301147]
  7. Province-Institute/Province-College Cooperation Project [201718016]
  8. SZSTI [JSGG20141020103826038]

Ask authors/readers for more resources

Hall-Petch relation was widely applied to evaluate the grain size effect on mechanical properties of metallic material. However, the sample size effect on the Hall-Petch relation was always ignored. In the present study, the mechanical test and microstructure observation were performed to investigate the combined effects of grain and sample sizes on the deformation behaviors of gold microwires. The polycrystalline gold microwires with diameter of 16 mu m were annealed at temperatures from 100 degrees C to 600 degrees C, leading to different ratios (t/d) of wire diameter (t) to grain size (d) from 0.9 to 16.7. When the t/d was lower than 10, the yield stress dropped fast and deviated from the Hall-Petch relation. The free-surface grains played key role in the yield stress softening, and the volume fraction of free-surface grains increased with the t/d decreasing. Furthermore, the effects of t/d on work-hardening behaviors and fracture modes were also studied. With t/d value decreasing from 17 to 3.4, the samples exhibited necking fracture and the dislocation pile-ups induced work-hardening stage was gradually activated. With the t/d value further decreasing (t/d < 3.4), the fracture mode turned into shear failure, and the work-hardening capability lost. As the gold microwire for wire bonding is commonly applied in the packaging of integrated circuit chips, and the fabrication of microwire suffers multi-pass cold-drawing and annealing treatments to control the grain size. The present study could provide instructive suggestion for gold microwire fabrication and bonding processes. (C) 2018 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.

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