Journal
ENVIRONMENTAL TECHNOLOGY
Volume 41, Issue 18, Pages 2400-2411Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/09593330.2019.1567607
Keywords
Characterization; modification; thermal decomposition; metal nanoparticles; Escherichia coli
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A new impregnation method was tested in this study. Without a stabilizing agent, silver and copper metallic compounds were directly impregnated on activated carbon using vacuum impregnation followed by drying at 100 degrees C and vacuum impregnation followed by thermal decomposition at 350 degrees C in an ambient atmosphere. The effect of thermal decomposition on the structural, morphological, and textural characteristics of the modified nanomaterials was analysed by Brunauer-Emmett-Teller, X-ray diffraction, scanning electron microscopy, energy dispersive X-Ray, and transmission electron microscopy. The characteristics of the produced materials were not altered. Silver and CuO nanoparticles were identified in the samples with average diameters ranging from 33.3-36.8 nm and 29.0-33.3 nm, respectively. The materials were tested for their antibacterial capacity and for their potential to leach Ag and Cu into water, thus analysing the effect of the thermal decomposition process on the impregnation process. The vacuum impregnation process followed by thermal decomposition produced the best results, with the resultant material reducing bacterial abundance by 5.31-6.61 log and leaching only low concentrations of metals into the water (Ag - 0.010-0.025 mg L-1 and Cu - 0.270-0.361 mg L-1). Samples produced without the thermal decomposition step reached bacterial reductions of 1.86-1.97 log and yielded higher concentrations of metals in the water (Ag - 0.051-0.086 mg L-1 and Cu - 0.819-0.894 mg L-1). [GRAPHICS]
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