Spatial and temporal exploration of heterogeneous catalysts with synchrotron radiation

Capturing the Genesis of an Active Fischer-Tropsch Synthesis Catalyst with Operando X-ray Nanospectroscopy

(2018) Ilse K. van Ravenhorst et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

In-Situ 2p3d Resonant Inelastic X-ray Scattering Tracking Cobalt Nanoparticle Reduction

(2017) Boyang Liu et al.   Journal of Physical Chemistry C

Supervised Machine-Learning-Based Determination of Three-Dimensional Structure of Metallic Nanoparticles

(2017) Janis Timoshenko et al.   Journal of Physical Chemistry Letters

High-resolution non-destructive three-dimensional imaging of integrated circuits

(2017) Mirko Holler et al.   NATURE

High-spatial-resolution mapping of catalytic reactions on single particles

(2017) Chung-Yeh Wu et al.   NATURE

Direct instrumental identification of catalytically active surface sites

(2017) Jonas H. K. Pfisterer et al.   NATURE

Beamstop-based low-background ptychography to image weakly scattering objects

(2017) Juliane Reinhardt et al.   ULTRAMICROSCOPY

A three-dimensional view of structural changes caused by deactivation of fluid catalytic cracking catalysts

(2017) J. Ihli et al.   Nature Communications

Time Resolved Operando X-ray Techniques in Catalysis, a Case Study: CO Oxidation by O2 over Pt Surfaces and Alumina Supported Pt Catalysts

(2017) Mark Newton   Catalysts

Development of a dose-limiting data collection strategy for serial synchrotron rotation crystallography

(2017) Kazuya Hasegawa et al.   JOURNAL OF SYNCHROTRON RADIATION

Chemical imaging of Fischer-Tropsch catalysts under operating conditions

(2017) Stephen W. T. Price et al.   Science Advances

In Situ Environmental TEM in Imaging Gas and Liquid Phase Chemical Reactions for Materials Research

(2016) Jianbo Wu et al.   ADVANCED MATERIALS

X-ray Excited Optical Fluorescence and Diffraction Imaging of Reactivity and Crystallinity in a Zeolite Crystal: Crystallography and Molecular Spectroscopy in One

(2016) Zoran Ristanović et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Visualizing Dealumination of a Single Zeolite Domain in a Real-Life Catalytic Cracking Particle

(2016) Sam Kalirai et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Liquid Cell Transmission Electron Microscopy

(2016) Hong-Gang Liao et al.   Annual Review of Physical Chemistry

Atomic-Scale Observations of Catalyst Structures under Reaction Conditions and during Catalysis

(2016) Franklin (Feng) Tao et al.   CHEMICAL REVIEWS

High spatial resolution mapping of chemically-active self-assembled N-heterocyclic carbenes on Pt nanoparticles

(2016) Y. Levratovsky et al.   FARADAY DISCUSSIONS

In Situ Ptychography of Heterogeneous Catalysts using Hard X-Rays: High Resolution Imaging at Ambient Pressure and Elevated Temperature

(2016) Sina Baier et al.   MICROSCOPY AND MICROANALYSIS

A MEMS-based heating holder for the direct imaging of simultaneousin-situheating and biasing experiments in scanning/transmission electron microscopes

(2016) Luigi Mele et al.   MICROSCOPY RESEARCH AND TECHNIQUE

In situ observation of self-assembled hydrocarbon Fischer–Tropsch products on a cobalt catalyst

(2016) Violeta Navarro et al.   Nature Chemistry

To get the most out of high resolution X-ray tomography: A review of the post-reconstruction analysis

(2016) Yijin Liu et al.   SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY

Current status and future directions for in situ transmission electron microscopy

(2016) Mitra L. Taheri et al.   ULTRAMICROSCOPY

Nanoscale Chemical Imaging of an Individual Catalyst Particle with Soft X-ray Ptychography

(2016) Anna M. Wise et al.   ACS Catalysis

X-ray spectroscopic and scattering methods applied to the characterisation of cobalt-based Fischer–Tropsch synthesis catalysts

(2016) Jennifer J. Herbert et al.   Catalysis Science & Technology

Active phase distribution changes within a catalyst particle during Fischer–Tropsch synthesis as revealed by multi-scale microscopy

(2016) K. H. Cats et al.   Catalysis Science & Technology

Influence of gas atmospheres and ceria on the stability of nanoporous gold studied by environmental electron microscopy and in situ ptychography

(2016) Sina Baier et al.   RSC Advances

High spatial resolution mapping of chemically-active self-assembled N-heterocyclic carbenes on Pt nanoparticles

(2016) Y. Levratovsky et al.   FARADAY DISCUSSIONS

Quick-EXAFS setup at the SuperXAS beamline forin situX-ray absorption spectroscopy with 10 ms time resolution

(2016) Oliver Müller et al.   JOURNAL OF SYNCHROTRON RADIATION

X-ray Fluorescence Tomography of Aged Fluid-Catalytic-Cracking Catalyst Particles Reveals Insight into Metal Deposition Processes

(2015) Sam Kalirai et al.   ChemCatChem

Real time chemical imaging of a working catalytic membrane reactor during oxidative coupling of methane

(2015) A. Vamvakeros et al.   CHEMICAL COMMUNICATIONS

Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

(2015) F. Meirer et al.   CHEMICAL COMMUNICATIONS

Fluid catalytic cracking: recent developments on the grand old lady of zeolite catalysis

(2015) E. T. C. Vogt et al.   CHEMICAL SOCIETY REVIEWS

Mapping Metals Incorporation of a Whole Single Catalyst Particle Using Element Specific X-ray Nanotomography

(2015) Florian Meirer et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Chemical imaging of single catalyst particles with scanning μ-XANES-CT and μ-XRF-CT

(2015) S. W. T. Price et al.   PHYSICAL CHEMISTRY CHEMICAL PHYSICS

Beyond crystallography: Diffractive imaging using coherent x-ray light sources

(2015) J. Miao et al.   SCIENCE

Opportunities and challenges in liquid cell electron microscopy

(2015) F. M. Ross   SCIENCE

Room-temperature carbon monoxide oxidation by oxygen over Pt/Al2O3 mediated by reactive platinum carbonates

(2015) Mark A. Newton et al.   Nature Communications

Comparative in Operando Studies in Heterogeneous Catalysis: Atomic and Electronic Structural Features in the Hydrogenation of Ethylene over Supported Pd and Pt Catalysts

(2015) Ulrich Jung et al.   ACS Catalysis

The potential of future light sources to explore the structure and function of matter

(2015) Edgar Weckert   IUCrJ

Life and death of a single catalytic cracking particle

(2015) F. Meirer et al.   Science Advances

Mapping Platinum Species in Polymer Electrolyte Fuel Cells by Spatially Resolved XAFS Techniques

(2014) Shinobu Takao et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

In situ X-ray ptychography imaging of high-temperature CO2 acceptor particle agglomerates

(2014) Kristin Høydalsvik et al.   APPLIED PHYSICS LETTERS

Catalytic Adventures in Space and Time Using High Energy X-rays

(2014) Mark A. Newton et al.   CATALYSIS SURVEYS FROM ASIA

Assessment of the 3 D Pore Structure and Individual Components of Preshaped Catalyst Bodies by X-Ray Imaging

(2014) Julio C. da Silva et al.   ChemCatChem

In Situ IR and X-ray High Spatial-Resolution Microspectroscopy Measurements of Multistep Organic Transformation in Flow Microreactor Catalyzed by Au Nanoclusters

(2014) Elad Gross et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Chemical composition mapping with nanometre resolution by soft X-ray microscopy

(2014) David A. Shapiro et al.   Nature Photonics

A review of advanced catalyst development for Fischer–Tropsch synthesis of hydrocarbons from biomass derived syn-gas

(2014) Hessam Jahangiri et al.   Catalysis Science & Technology

Correlating Metal Poisoning with Zeolite Deactivation in an Individual Catalyst Particle by Chemical and Phase-Sensitive X-ray Microscopy

(2013) Javier Ruiz-Martínez et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Nanoscale Hard X-Ray Microscopy Methods for Materials Studies

(2013) Martin Holt et al.   Annual Review of Materials Research

Fischer–Tropsch synthesis: Activity of metallic phases of cobalt supported on silica

(2013) Muthu Kumaran Gnanamani et al.   CATALYSIS TODAY

Single-catalyst particle spectroscopy of alcohol-to-olefins conversions: Comparison between SAPO-34 and SSZ-13

(2013) Qingyun Qian et al.   CATALYSIS TODAY

X-ray nanoscopy of cobalt Fischer–Tropsch catalysts at work

(2013) Korneel H. Cats et al.   CHEMICAL COMMUNICATIONS

Reactivity of Surface Species in Heterogeneous Catalysts Probed by In Situ X-ray Absorption Techniques

(2013) Silvia Bordiga et al.   CHEMICAL REVIEWS

Single-Particle Spectroscopy on Large SAPO-34 Crystals at Work: Methanol-to-Olefin versus Ethanol-to-Olefin Processes

(2013) Qingyun Qian et al.   CHEMISTRY-A EUROPEAN JOURNAL

Hard X-ray Spectroscopic Nano-Imaging of Hierarchical Functional Materials at Work

(2013) Joy C. Andrews et al.   CHEMPHYSCHEM

From Grain Boundaries to Single Defects: A Review of Coherent Methods for Materials Imaging in the X-ray Sciences

(2013) Brian Abbey   JOM

In Situ TEM Study of Catalytic Nanoparticle Reactions in Atmospheric Pressure Gas Environment

(2013) Huolin L. Xin et al.   MICROSCOPY AND MICROANALYSIS

Catalysts for Production of Lower Olefins from Synthesis Gas: A Review

(2013) Hirsa M. Torres Galvis et al.   ACS Catalysis

Hard X-ray Nanotomography of Catalytic Solids at Work

(2012) Ines D. Gonzalez-Jimenez et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

A combined in situ XAS-XRPD-Raman study of Fischer–Tropsch synthesis over a carbon supported Co catalyst

(2012) Nikolaos E. Tsakoumis et al.   CATALYSIS TODAY

Imaging Catalysts at Work: A Hierarchical Approach from the Macro- to the Meso- and Nano-scale

(2012) Jan-Dierk Grunwaldt et al.   ChemCatChem

Porous materials in catalysis: challenges for mesoporous materials

(2012) Carlo Perego et al.   CHEMICAL SOCIETY REVIEWS

Iron Particle Size Effects for Direct Production of Lower Olefins from Synthesis Gas

(2012) Hirsa M. Torres Galvis et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Structure and acidity of individual Fluid Catalytic Cracking catalyst particles studied by synchrotron-based infrared micro-spectroscopy

(2012) Inge L.C. Buurmans et al.   MICROPOROUS AND MESOPOROUS MATERIALS

Heterogeneities of individual catalyst particles in space and time as monitored by spectroscopy

(2012) Inge L. C. Buurmans et al.   Nature Chemistry

The Porosity, Acidity, and Reactivity of Dealuminated Zeolite ZSM-5 at the Single Particle Level: The Influence of the Zeolite Architecture

(2011) Luis R. Aramburo et al.   CHEMISTRY-A EUROPEAN JOURNAL

Recent developments in dynamic transmission electron microscopy

(2011) N.D. Browning et al.   CURRENT OPINION IN SOLID STATE & MATERIALS SCIENCE

Femtosecond X-ray protein nanocrystallography

(2011) Henry N. Chapman et al.   NATURE

Electron microscopy of specimens in liquid

(2011) Niels de Jonge et al.   Nature Nanotechnology

The Race to X-ray Microbeam and Nanobeam Science

(2011) G. E. Ice et al.   SCIENCE

Using X-Ray Microtomography for Characterisation of Catalyst Particle Pore Structure

(2010) Luca Ruffino et al.   CANADIAN JOURNAL OF CHEMICAL ENGINEERING

Deactivation of cobalt based Fischer–Tropsch catalysts: A review

(2010) Nikolaos E. Tsakoumis et al.   CATALYSIS TODAY

Analysing and understanding the active site by IR spectroscopy

(2010) Alexandre Vimont et al.   CHEMICAL SOCIETY REVIEWS

Chemical imaging of catalytic solids with synchrotron radiation

(2010) Andrew M. Beale et al.   CHEMICAL SOCIETY REVIEWS

Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales

(2010) Jan-Dierk Grunwaldt et al.   CHEMICAL SOCIETY REVIEWS

Infrared and Raman imaging of heterogeneous catalysts

(2010) Eli Stavitski et al.   CHEMICAL SOCIETY REVIEWS

Probing the surfaces of heterogeneous catalysts by in situ IR spectroscopy

(2010) Carlo Lamberti et al.   CHEMICAL SOCIETY REVIEWS

In-situ Scanning Transmission X-Ray Microscopy of Catalytic Solids and Related Nanomaterials

(2010) Frank M. F. de Groot et al.   CHEMPHYSCHEM

Transmission X-ray microscopy for full-field nano imaging of biomaterials

(2010) Joy C. Andrews et al.   MICROSCOPY RESEARCH AND TECHNIQUE

Nanoscale X-ray imaging

(2010) Anne Sakdinawat et al.   Nature Photonics

First steps in combining modulation excitation spectroscopy with synchronous dispersive EXAFS/DRIFTS/mass spectrometry for in situ time resolved study of heterogeneous catalysts

(2010) Davide Ferri et al.   PHYSICAL CHEMISTRY CHEMICAL PHYSICS

High-resolution projection image reconstruction of thick objects by hard x-ray diffraction microscopy

(2010) Yukio Takahashi et al.   PHYSICAL REVIEW B

Label-Free Chemical Imaging of Catalytic Solids by Coherent Anti-Stokes Raman Scattering and Synchrotron-Based Infrared Microscopy

(2009) Marianne���H.���F. Kox et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Probing Solid Catalysts under Operating Conditions: Electrons or X-rays?

(2009) John Meurig Thomas et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Nanoscale Chemical Imaging of the Reduction Behavior of a Single Catalyst Particle

(2009) Emiel de Smit et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Chemical Imaging of Spatial Heterogeneities in Catalytic Solids at Different Length and Time Scales

(2009) Bert M. Weckhuysen   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Spatiotemporal Multitechnique Imaging of a Catalytic Solid in Action: Phase Variation and Volatilization During Molybdenum Oxide Reduction

(2009) Matthew G. O'Brien et al.   ChemCatChem

On the Origin of the Cobalt Particle Size Effects in Fischer−Tropsch Catalysis

(2009) J. P. den Breejen et al.   JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

Morphology-dependent zeolite intergrowth structures leading to distinct internal and outer-surface molecular diffusion barriers

(2009) Lukasz Karwacki et al.   NATURE MATERIALS

Breaking the 10 nm barrier in hard-X-ray focusing

(2009) Hidekazu Mimura et al.   Nature Physics

Demonstration of 12 nm Resolution Fresnel Zone Plate Lens based Soft X-ray Microscopy

(2009) Weilun Chao et al.   OPTICS EXPRESS

In Situ Synchrotron-Based IR Microspectroscopy To Study Catalytic Reactions in Zeolite Crystals

(2008) Eli Stavitski et al.   ANGEWANDTE CHEMIE-INTERNATIONAL EDITION

Fischer–Tropsch Synthesis: Reaction mechanisms for iron catalysts

(2008) Burtron H. Davis   CATALYSIS TODAY

Catalysts at work: From integral to spatially resolved X-ray absorption spectroscopy

(2008) Jan-Dierk Grunwaldt et al.   CATALYSIS TODAY

The renaissance of iron-based Fischer–Tropsch synthesis: on the multifaceted catalyst deactivation behaviour

(2008) Emiel de Smit et al.   CHEMICAL SOCIETY REVIEWS

Deactivation of FCC catalysts

(2008) H.S. Cerqueira et al.   JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL

Nanoscale chemical imaging of a working catalyst by scanning transmission X-ray microscopy

(2008) Emiel de Smit et al.   NATURE

Coherent X-Ray Diffraction Imaging with Nanofocused Illumination

(2008) C. G. Schroer et al.   PHYSICAL REVIEW LETTERS

Atomic-scale electron microscopy at ambient pressure

(2008) J.F. Creemer et al.   ULTRAMICROSCOPY