Journal
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY
Volume 8, Issue 2, Pages 434-439Publisher
SCIENDO
DOI: 10.2478/s11532-010-0007-1
Keywords
Nickel; Nanothorns; Self-assembly; Field-emission scanning electron microscopy; Magnetic property
Categories
Funding
- Jiangsu University of Science and Technology [35060810]
- university in Jiangsu [09KJD430006]
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Hierarchical nickel microwires with nanothorns were fabricated through a reduction of nickelous salt with hydrazine in diethanolamine. The product was characterized by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), and energy-dispersive X-ray spectroscopy (EDS). The growth mechanism of the nickel microwires with nanothorns is proposed, based on the evolution of the structures and morphologies, which could be ascribed to the cooperative effect of the complexant of diethanolamine and inherent magnetic interactions. Magnetic properties of the product were measured at room temperature and compared with other shaped counterparts.
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