Journal
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY
Volume 7, Issue 3, Pages 555-559Publisher
DE GRUYTER POLAND SP Z O O
DOI: 10.2478/s11532-009-0049-4
Keywords
Ionic liquids; Nanoparticles; Mn3O4; [BMIM]OH; TEM; EPR
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Funding
- Fatih University Research Project Foundation [P50020803-2]
- Turkish Ministry of Industry and Trade [00185. STZ.2007-2]
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A novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn3O4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmission electron microscopy. Phase purity was confirmed by XRD, and X-ray line profile fitting determined a crystallite size of 42 +/- 11 nm. TEM analysis revealed various morphologies. EPR measurements have indicated the existence of long-range interactions, due to the wide range of particle sizes and morphologies observed
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