4.6 Article

Localized Overheating Phenomena and Optimization of Spark-Plasma Sintering Tooling Design

Journal

MATERIALS
Volume 6, Issue 7, Pages 2612-2632

Publisher

MDPI
DOI: 10.3390/ma6072612

Keywords

Spark Plasma Sintering (SPS); Field Assisted Sintering (FAST); finite element; modeling; temperature distribution; overheating

Funding

  1. US ARDEC, Picatinny Arsenal [W15QKN-09C-0128]
  2. Department of Energy Division of Materials Sciences and Engineering (DOE) [DE-SC0008581]
  3. Department of Science and Education of Russian Federation [11.G34.31.0051]
  4. Directorate For Engineering
  5. Div Of Civil, Mechanical, & Manufact Inn [0758232] Funding Source: National Science Foundation

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The present paper shows the application of a three-dimensional coupled electrical, thermal, mechanical finite element macro-scale modeling framework of Spark Plasma Sintering (SPS) to an actual problem of SPS tooling overheating, encountered during SPS experimentation. The overheating phenomenon is analyzed by varying the geometry of the tooling that exhibits the problem, namely by modeling various tooling configurations involving sequences of disk-shape spacers with step-wise increasing radii. The analysis is conducted by means of finite element simulations, intended to obtain temperature spatial distributions in the graphite press-forms, including punches, dies, and spacers; to identify the temperature peaks and their respective timing, and to propose a more suitable SPS tooling configuration with the avoidance of the overheating as a final aim. Electric currents-based Joule heating, heat transfer, mechanical conditions, and densification are imbedded in the model, utilizing the finite-element software COMSOL (TM), which possesses a distinguishing ability of coupling multiple physics. Thereby the implementation of a finite element method applicable to a broad range of SPS procedures is carried out, together with the more specific optimization of the SPS tooling design when dealing with excessive heating phenomena.

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