Journal
ACS CATALYSIS
Volume 3, Issue 12, Pages 3002-3005Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cs4009336
Keywords
iron; sulfur; catalysis; addition; carbene ligand
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A defined NHC-Fe-S complex proved to be an efficient catalyst for the selective hydrosulfenylation of alpha/beta-unsaturated ketones or vinylnitriles. A wide range of different aliphatic thiols were transferred in this atom-economic reaction into the corresponding thioethers. Mild reaction conditions, equimolar amounts of substrates, low catalyst loadings, and mild reaction conditions are characteristic for this transformation.
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