Journal
JOURNAL OF CHEMICAL RESEARCH
Volume -, Issue 6, Pages 358-360Publisher
SAGE PUBLICATIONS LTD
DOI: 10.3184/030823410X12744466896732
Keywords
trichloroisocyanuric acid (TCCA); disulfides; thiosulfonates; solvent-free synthesis
Categories
Funding
- National Key Technology RD Program [2007BAI34B00]
- Natural Science Foundation of Zhejiang Province [Y4080107]
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Trichloroisocyanuric acid (TCCA) is an inexpensive and efficient reagent for solvent-free chemoselective synthesis of thiosulfonates by grinding, providing a metal-free new methodology for the oxidation of disulfides. The important features of this method are that it is reasonably fast, very clean, high yielding, has a simple workup and is environmentally benign.
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