Journal
TETRAHEDRON LETTERS
Volume 54, Issue 1, Pages 66-71Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.10.094
Keywords
Diacetylene; Ferrocene; Dimethylaminobenzene; Proton; Integrated reaction; Conformation; Control
Categories
Funding
- Ministry of Education, Science, Sports, Culture and Technology [22106512, 23550046]
- Grants-in-Aid for Scientific Research [23550046, 24550151, 22106512] Funding Source: KAKEN
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An extended pi-electronic conjugation system of the 1,1'-bis[p-(N,N-dimethylaminophenyl)butadiynyl]ferrocene derivative 1 has been synthesized, with our integrated cross-coupling reaction between the corresponding TMS-protected acetylenes in one-pot. Quantitative H-1 NMR and UV-vis spectral studies of 1 have been performed, providing a methodology for molecular functions transformable by a proton-mediated reversible conformation control. (C) 2012 Elsevier Ltd. All rights reserved.
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