Journal
TETRAHEDRON LETTERS
Volume 54, Issue 1, Pages 101-105Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.10.114
Keywords
lodobenzene; Oxone (R); Tetrazole; Triazole; Desulfurization
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Funding
- University Grant Commission (UGC) India
- Rajiv Gandhi National Fellowship (RGNF)
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A novel and expedient regioselective method for the synthesis of 5-aminotetrazoles and 3-amino-1,2,4-triazoles through oxidative desulfurization of corresponding 1,3-disubstituted thioureas has been discovered and optimized for the process conditions. The process is broadly applicable to structurally diverse 1,3-disubstituted thioureas. (C) 2012 Elsevier Ltd. All rights reserved.
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