Journal
TETRAHEDRON LETTERS
Volume 53, Issue 38, Pages 5171-5175Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.07.057
Keywords
Carbonylation; Alkenyl tosylates; Phenyl formate; Palladium
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Funding
- Daiichi-Sankyo Co., Ltd.
- Grants-in-Aid for Scientific Research [23790016] Funding Source: KAKEN
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Palladium-catalyzed carbonylation of tosylates with phenyl formate is described. This procedure needs neither external carbon monoxide nor any pressure-resistant apparatus. A variety of cyclic and acyclic alkenyl tosylates can be converted into the corresponding phenyl esters in good yields. Furthermore, this method is effective for the one-pot synthesis of alpha,beta-unsaturated amides. (C) 2012 Elsevier Ltd. All rights reserved.
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