Journal
TETRAHEDRON LETTERS
Volume 53, Issue 32, Pages 4173-4178Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2012.05.142
Keywords
Microwave-assisted synthesis; Macrocycle; Diaryl ether; Intramolecular; Bimolecular; Ullmann coupling
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Funding
- NIH Academic Research Enhancement Award (AREA) [R15AI092315]
- UHH CoP startup funds
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Microwave-assisted synthesis of macrocyclic diaryl ethers via intramolecular and/or bimolecular Ullmann coupling is described. Using the optimized conditions, a panel of macrocycles, with different substitution patterns, ring sizes, and linkers, has been successfully synthesized using microwave irradiation. To the best of our knowledge, this work represents the first examples of the microwave-assisted synthesis of macrocyclic diaryl ethers via intramolecular and/or bimolecular Ullmann coupling. (C) 2012 Elsevier Ltd. All rights reserved.
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