Journal
TETRAHEDRON LETTERS
Volume 50, Issue 49, Pages 6810-6813Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2009.09.107
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Funding
- NIH [P50-GM067082]
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Microwave irradiation facilitated the synthesis of 4-arylthio-3-oxazolin-5-ones front ethyl cyanoformate, thiophenol, and cyclic ketones. Subsequent decarboxylation and in Situ [3+2] cycloaddition provided novel 2,3,4,5-tetrahydro-1H-pyrrolo[1,2-c][1,3]diazepine scaffolds after a spontaneous retro-Mannich domino reaction. (C) 2009 Elsevier Ltd. All rights reserved.
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