Journal
TETRAHEDRON
Volume 69, Issue 16, Pages 3459-3464Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2013.02.059
Keywords
Cyclizations; Dianions; Organofluorine compounds; Tautomerism; 1,3,5-Tricarbonyl compounds
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Funding
- State of Mecklenburg-Vorpommern
- EU (EFRE program)
- Volkswagenstiftung [Az86223]
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The cyclization of fluoroalkylated 3,5-dioxoesters with hydrazines, carried out in glacial acetic acid, afforded pyrazines with fluoroalkylated side-chain. The cyclization of 3,5-dioxoesters with hydroxylamine afforded hydroxylated fluoroalkylated dihydroisoxazoles. All reactions proceeded with good to very good regioselectivity. (C) 2013 Elsevier Ltd. All rights reserved.
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