Journal
TETRAHEDRON
Volume 67, Issue 47, Pages 9099-9103Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.09.082
Keywords
Palladium-catalyzed; Suzuki-Miyaura coupling; 6-Chloropurines; Sodium tetraarylborate; Water; Microwave-assisted synthesis
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Funding
- National Nature Science Foundation of China [20802016, 21072047]
- Ministry of Education [NCET-09-0122]
- Excellent Youth Foundation of Henan Scientific Committee [114100510012]
- Program for Changjiang Scholars and Innovative Research Team in University [IRT1061]
- National Students Innovation Experiment Program
- Henan Normal University
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An efficient method for the synthesis of 6-arylpurines (nucleosides) was developed via Suzuki-Miyaura cross-coupling reactions of 6-chloropurines (nucleosides) and sodium tetraarylborate in neat water (ethanol). The process gave good to high isolated yields within a short reaction time under microwave irradiated conditions. (C) 2011 Elsevier Ltd. All rights reserved.
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