Journal
TETRAHEDRON
Volume 65, Issue 37, Pages 7790-7793Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.07.036
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Funding
- Natural Science Foundation of China [NSFC 20602011]
- Shanghai Committee of Science and Technology [06PJ14023]
- New Century Excellent Talents in University, the Ministry of Education, China [NCET-07-0283]
- '111' Project [B07023]
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TsCl (p-toluenesulfonyl chloride), a commercially available organosulfonyl chloride, has been widely used as a stoichiometric dehydrogenation reagent in the transformation of ketoximes into corresponding amides via the Beckmann rearrangement. It has been now found to catalyze the Beckmann rearrangement with high catalytic efficiency, converting a wide range of ketoximes into their corresponding amides under mild condition with good to excellent yields (up to 99% of yield with 1-5 mol% of catalyst loading). (C) 2009 Elsevier Ltd. All rights reserved.
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