Journal
SYNTHESIS-STUTTGART
Volume -, Issue 11, Pages 1771-1776Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1218730
Keywords
Beckmann rearrangement; ketoximes; amides; bromodimethylsulfonium bromide (BDMS); catalytic process; Lewis acids
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Funding
- CSIR, New Delhi
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Bromodimethylsulfonium bromide, in combination with zinc chloride, has been shown to be an excellent catalytic system for liquid-phase Beckmann rearrangement of various ketoximes into the corresponding amides/lactams in acetonitrile at reflux temperature with good to excellent yields.
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