Journal
SYNLETT
Volume -, Issue 19, Pages 2886-2890Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0031-1289872
Keywords
room temperature; metal-free; 1,1-dithio-1-alkenes; 1,1-dibromo-1-alkenes; thiols
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Funding
- Natural Science Foundation of China [30873153]
- Key Projects of Shanghai in Biomedical [08431902700]
- Scientific Research Foundation of State Education Ministry for the Returned Overseas Chinese Scholars
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An efficient metal-free synthesis of 1,1-dithio-1-alkenes from 1,1-dibromo-1-alkenes and thiols using a diazabicycloundecene/dimethyl sulfoxide system was developed. The method was found suitable for various 1,1-dibromo-1-alkenes. The synthesis was completed within 5-15 minutes at room temperature with moderate to excellent yields.
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