Journal
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
Volume 53, Issue 7, Pages 1000-1005Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023608070048
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Unsolvated aluminum hydride has been synthesized by the direct reaction of aluminum bromide or sulfuric acid with an alkali metal tetrahydroaluminate at 90-102 degrees C in pure toluene or in toluene containing 5-10 wt % diethyl ether. The reaction involving aluminum bromide yields a mixture of unsolvated aluminum hydride phases of poor quality. The reaction with sulfuric acid affords a single-phase product as alpha-AlH3 at <= 90 degrees C.
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