4.5 Article

Note: Grazing incidence small and wide angle x-ray scattering combined with imaging ellipsometry

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 83, Issue 7, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.4738880

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Funding

  1. Bundesministerium fur Bildung und Forschung [05KS7WO1]
  2. Bavarian State Ministry of Sciences, Research and Arts through the International Graduate School Materials Science of Complex Interfaces
  3. Erasmus Mundus MaMa-SELF program

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The combination of grazing incidence small angle x-ray scattering (GISAXS) and grazing incidence wide angle x-ray scattering (GIWAXS) with optical imaging ellipsometry is presented as an upgrade of the available measurement techniques at the wiggler beamline BW4 of the Hamburger Synchrotronstrahlungslabor. The instrument is introduced with the description of the alignment procedure to assure the measurement of imaging ellipsometry and GISAXS/GIWAXS on the same sample spot. To demonstrate the possibilities of the new instrument examples of morphological investigation on films made of poly(3-hexylthiophene) and [6,6]-phenyl-C-61 butyric acid methyl ester as well as textured poly(9,9-dioctylfluorene-alt-benzo-thia-diazole) are shown. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.4738880]

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