Journal
ACS COMBINATORIAL SCIENCE
Volume 17, Issue 9, Pages 483-487Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acscombsci.5b00086
Keywords
resin-bound triphenylphosphine; selectivity; monoesterification; amides; symmetrical diols; 4-DMAP
Funding
- SERB, Department of Science and Technology (DST), Govt. of India, New Delhi [SB/FT/CS-103/2013]
- TEQIP-II, NIT Silchar
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Coupling reactions to make esters and amides are among the most widely used organic transformations. We report efficient procedures for amide bond formation and for the monoesterification of symmetrical diols in excellent yields without any requirement for high dilution or slow addition using resin-bound triarylphosphonium iodide. Easy purification, low moisture sensitivity, and good to excellent yields of the products are the major advantages of this protocol.
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