Journal
POWDER TECHNOLOGY
Volume 206, Issue 3, Pages 214-217Publisher
ELSEVIER
DOI: 10.1016/j.powtec.2010.09.015
Keywords
Mesoporous; Solventless template removal; Sublimation; Menthol template; Nonsurfactant template; Organosilica
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Menthol templated vinyl-functionalized organosilica materials were prepared by acid catalyzed hydrolytic sol-gel reactions of tetraethyl orthosilicate and vinyltriethoxysilane. The menthol template was removed by sublimation under vacuum, leading to the formation of a mesoporous organosilica material. This work presents a solventless, low temperature method of extraction of template from mesoporous materials. For the first time, sublimation was demonstrated to be an effective means of template removal to generate a mesoporous material. A comparison of sublimation and solvent extraction as template removal methods is also presented. (C) 2010 Elsevier B.V. All rights reserved.
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