Journal
ORGANIC LETTERS
Volume 20, Issue 17, Pages 5219-5223Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b02168
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Funding
- Spanish MINECO [CTQ2015-64624-R]
- European Regional Development Fund/European Social Fund
- FUSP-CEU [PC17/17]
- Fundacion San Pablo-CEU
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Cobalt-catalyzed alkyne cyclotrimerization and crossed [2 + 2 + 2] cycloadditions are developed in a plug flow reactor. The protocol generally uses 5 mol % of Co-2(CO)(8) and is scalable at least at multigram scale. Efficient and scalable use of Co-2(CO)(8) for crossed reactions of diynes and alkynes has hardly any precedent.
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