Journal
ORGANIC LETTERS
Volume 15, Issue 22, Pages 5842-5845Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol402904d
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Funding
- Welch Foundation [E-1571]
- NIGMS [R01GM077635]
- Camille and Henry Dreyfus Foundation
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A method for direct, auxiliary-assisted alkoxylation and phenoxylation of beta-sp(2) C-H bonds of benzoic acid derivatives and gamma-sp(2) C-H bonds of amine derivatives is reported. The reaction employs (CuOH)(2)CO3 catalyst, air as an oxidant, phenol or alcohol coupling partner, DMF, pyridine, or DMPU solvent, and K2CO3, tetramethylguanidine, or K3PO4 base at 70-130 degrees C.
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