Journal
ORGANIC LETTERS
Volume 14, Issue 22, Pages 5784-5787Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol302852q
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- University of Auckland
- Maurice Wilkins Centre for Molecular Biodiscovery
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The postulated structure of the potent anticancer peptaibol culicinin D has been synthesized using Fmoc-based solid-phase peptide synthesis (SPPS). Comparison of the H-1 NMR data for the reported structure of culicinin D with the data obtained for the two synthetic polypeptides epimeric at C-6 in the AHMOD unit established the C-6 stereochemistry of the AHMOD residue in the natural product to be (R).
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