Journal
ORGANIC LETTERS
Volume 14, Issue 3, Pages 862-865Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol203388j
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Azine N-oxides undergo highly regioselective metalation with TMPZnCl center dot LiCl under mild conditions. A palladium-catalyzed Negishi cross-coupling reaction of the resulting organozinc species with heteroaromatic bromides provides heterobiaryls specifically oxidized at one nitrogen position in up to 95% yield.
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