Journal
ORGANIC LETTERS
Volume 14, Issue 12, Pages 2929-2931Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol301092w
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Funding
- National Science Foundation [CHE-0806356]
- Direct For Mathematical & Physical Scien [0806356, 0840521] Funding Source: National Science Foundation
- Division Of Chemistry [0806356, 0840521] Funding Source: National Science Foundation
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An acid-catalyzed intramolecular [4 + 2] cycloaddition of a non-natural bisabolene is reported. The key cyclocondensation was developed to access cyclic sesquiterpenes from linear phenolic precursors by generating a reactive o-quinone methide intermediate to initiate a cascade reaction. The new method was applied to the first total synthesis of (+/-)-heliol.
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