Journal
ORGANIC LETTERS
Volume 14, Issue 5, Pages 1187-1189Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol300272j
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Funding
- FPU [AP20090051]
- Spanish government (MICINN) [CTQ2010-16170]
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A new stereoselective tandem reaction consisting of the metal-free conjugate addition of boronic acids followed by an intramolecular ring opening of a cyclic acetal has been disclosed. Optically pure polysubstituted tetrahydropyrans have been synthesized diastereoselectively by this new reaction. Two new C C bonds and up to three stereocenters are formed in a single step, allowing the generation of quaternary stereocenters.
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