Journal
ORGANIC LETTERS
Volume 13, Issue 5, Pages 1098-1101Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol103130s
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The highly regio- and stereoselective 6-exo-dig mode cyclization of N-acyl-o-alkynylanilines producing 4-alkylidene-3,1-benzoxazines occurred unpredictably by use of a proper catalyst [Pd(OAc)(2)] and an effective additive (acetic acid) under suitable reaction conditions.
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