Journal
ORGANIC LETTERS
Volume 13, Issue 22, Pages 6122-6125Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol2026125
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Funding
- National Institutes of Health [GM 46503]
- National Science Foundation [CHE-0748121]
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The synthesis of N-aryl-2-carboxyl-3-hydroxy-5-arylpyrroles has been achieved in high yield by the combination of a TBSO-substituted vinyldiazoacetate and nitrones in a one-pot cascade process involving copper-catalyzed Mannich addition, dirhodium-catalyzed dinitrogen extrusion and N-OTBS insertion, and acid-promoted aromatization (elimination).
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