Journal
ORGANIC LETTERS
Volume 11, Issue 20, Pages 4728-4731Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol901867q
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Funding
- Korea Sanhak Foundation [2009-77]
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A general approach for the synthesis of novel 2-fluoro-3-phenylthio-1,3-butadiene (8) and 2-trifluoromethyl-3-phenylthio-1,3-butadiene (9) from monobromoalkene and dibromoalkenes has been developed. Subsequent Diels-Alder reactions of these dienes with symmetrical and unsymmetrical dienophiles in the presence of Lewis acids gave a variety of fluorinated six-membered carbocycles in moderate to high yields.
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