Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 12, Issue 43, Pages 8603-8606Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ob01736f
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Funding
- National Natural Science Foundation of China [21074054, 21172106, 21372114]
- National Basic Research Program of China [2010CB923303]
- Research Fund for the Doctoral Program of Higher Education of China [20120091110010]
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A rhodium-catalyzed ortho-cyanation of symmetrical azobenzenes is described employing N-cyano-N-phenyl-p-toluenesulfonamide as an environmentally friendly cyanide source. The present protocol allows the synthesis of various benzonitrile derivatives in moderate to good yields and tolerates many useful functional groups.
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