Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 23, Pages 8119-8121Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ob06300f
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Funding
- MEST [NRF-20090085824, NRF-2010-0029698, 2011-0001334, R31-2008-10029]
- Korea Research Council Industrial Science and Technology [B551179-10-03-00]
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A mild and efficient protocol for the deprotection of silyl ethers using KF in tetraethylene glycol is reported. A wide range of alcoholic silyl ethers can be selectively cleaved in high yield in the presence of certain acid- and base-labile functional groups. Moreover, the phenolic silyl ethers were cleaved exclusively, without affecting the alcoholic silyl ethers, at room temperature.
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