Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 7, Pages 2062-2064Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ob01148g
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Funding
- Ministry of Education, Culture, Sports, Science and Technology of Japan
- Japan Private School Promotion Foundation
- Research Foundation for Pharmaceutical Sciences
- Grants-in-Aid for Scientific Research [22790028] Funding Source: KAKEN
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Direct generation of a benzyl radical by C-H bond activation of toluenes and the addition reaction of the resulting radical to an electron deficient olefin were developed. The reaction of dimethyl fumarate with toluene in the presence of Et3B as a radical initiator at reflux afforded 2-benzylsuccinic acid dimethyl ester in good yield.
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