Journal
TETRAHEDRON LETTERS
Volume 56, Issue 41, Pages 5656-5660Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.08.066
Keywords
Iron catalyzed; Amide; Amine; Aldehyde; Oxidation
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Funding
- University Grants Commission (UGC), New Delhi
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An environmentally friendly synthetic route by the application of CO2 to synthesize amides via in situ protection and deprotection of amines for iron catalyzed oxidative amidation of aldehydes was developed. Various secondary and tertiary amides have been synthesized in moderate to good yields under mild and neutral reaction conditions. The use of amine hydrochloride salts and hence base for neutralization step is totally avoided in this protocol. (C) 2015 Elsevier Ltd. All rights reserved.
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