Journal
SYNTHETIC COMMUNICATIONS
Volume 45, Issue 13, Pages 1546-1551Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2015.1031249
Keywords
2-Amino-4H-chromenes; green reaction; malononitrile; phloroglucinol; resorcinol
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Funding
- Royal Society of Chemistry
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The preparation of substituted 2-amino-4H-chromenes by a Na2CO3-catalyzed reaction of malononitrile, benzaldehydes, and phloroglucinol or resorcinol in aqueous medium and at room temperature is reported. The merits of this procedure include limited use of organic solvents, easy workup technique, and high purity of products. The 2-amino-4H-chromenes were prepared in yields of 54-96%.
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