Journal
SYNLETT
Volume 26, Issue 7, Pages 965-969Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0034-1380399
Keywords
solanoeclepin A; natural products; radical cyclization; iodoetherification; enyne metathesis
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Funding
- MEXT
- Yamada Science Foundation
- Daiichi Sankyo Foundation of Life Science
- SUNBOR GRANT from the Suntory Institute for Bioorganic Research
- Grants-in-Aid for Scientific Research [15K12743, 24580161, 15K07410, 23102015] Funding Source: KAKEN
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A tricyclic compound possessing oxabicyclo[2.2.1]heptane and seven-membered ring of solanoeclepin A, the most active hatching agent of potato cyst nematode, was synthesized from d-pantolactone. The synthesis features a tin-mediated 6-exo-trig radical cyclization followed by iodoetherification and ring-closing enyne metathesis.
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