Journal
MICROCHIMICA ACTA
Volume 181, Issue 13-14, Pages 1521-1527Publisher
SPRINGER WIEN
DOI: 10.1007/s00604-014-1208-7
Keywords
Quartz crystal microbalance; Gold nanoparticles; Signal amplification; Pb2+
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Funding
- National Natural Science Foundation of China [21375134, 21105105, 21135006, 21321003]
- Institute of Chemistry, Chinese Academy of Sciences [CMS-PY-201214]
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A novel quartz crystal microbalance (QCM) sensor has been developed for highly selective and sensitive detection of Pb2+ by exploiting the catalytic effect of Pb2+ ions on the leaching of gold nanoparticles from the surface of a QCM sensor. The use of self-assembled gold nanoparticles (AuNPs) strongly enlarges the size of the interface and thus amplifies the analytical response resulting from the loss of mass. This results in a very low detection limit for Pb2+ (30 nM). The high selectivity is demonstrated by studying the effect of potentially interfering ions both in the absence and presence of Pb2+ ions. This simple and well reproducible sensor was applied to the determination of lead in the spiked drinking water. This work provides a novel strategy for fabricating QCM sensors towards Pb2+ (i)n real samples.
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