4.5 Article

New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 86, Issue 7, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.4926895

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Funding

  1. DOE-NNSA [DE-NA0001974]
  2. DOE-BES [DE-FG02-99ER45775]
  3. NSF
  4. DOE Office of Science [DE-AC02-06CH11357]
  5. EFree, an Energy Frontier Research Center - DOE-BES

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An overview of the in situ laser heating system at the High Pressure Collaborative Access Team, with emphasis on newly developed capabilities, is presented. Since its establishment at the beamline 16-ID-B a decade ago, laser-heated diamond anvil cell coupled with in situ synchrotron x-ray diffraction has been widely used for studying the structural properties of materials under simultaneous high pressure and high temperature conditions. Recent developments in both continuous-wave and modulated heating techniques have been focusing on resolving technical issues of the most challenging research areas. The new capabilities have demonstrated clear benefits and provide new opportunities in research areas including high-pressure melting, pressure-temperature volume equations of state, chemical reaction, and time resolved studies. (C) 2015 AIP Publishing LLC.

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