Journal
MATERIALS RESEARCH BULLETIN
Volume 47, Issue 6, Pages 1609-1612Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2012.02.040
Keywords
Inorganic compounds; Chemical synthesis; X-ray diffraction; Electrochemical properties
Categories
Funding
- National Nature Science Foundation of China [20973124]
- Guangdong Sci. & Tech. Key Projects [2009A080208001]
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A fast sol-gel assisted microwave heating approach has been developed for the synthesis of high-rate Li3V2(PO4)(3)/C cathode material. This approach can synthesize Li3V2(PO4)(3)/C particles with high purity and good crystallinity in 12 min at a low microwave power of 320 W. In the voltage range of 3.0-4.3 V, the obtained Li3V2(PO4)(3)/C delivers a reversible discharge capacity of 100 mAh g(-1) after 100 cycles at 20 degrees C, exhibiting excellent rate capability and cycling performance. The rate-recovery performance also suggests that the Li3V2(PO4)(3)/C material possesses excellent structure stability after high-rate cycles, presenting excellent application value in high-power lithium ion batteries. (C) 2012 Elsevier Ltd. All rights reserved.
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