Journal
MACROMOLECULAR CHEMISTRY AND PHYSICS
Volume 214, Issue 19, Pages 2245-2249Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/macp.201300350
Keywords
ethylene copolymerization; NMR spectroscopy; polar monomers; Ziegler-Natta polymerization
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Copolymerization of ethylene with 4-penten-1-ol (4P1O) is conducted by using a half-titanocene catalyst. The incorporation of 4P1O is high as approximately 10 mol%. The assignments of the C-13 NMR spectrum and the analysis of the sequence distribution show the existence of not only the alternative structure but also the repeated 4P1O units. The product of the reactive ratios is calculated as ca. 2.
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